کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5010095 | 1462050 | 2017 | 10 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis of the porous NiO/SnO2 microspheres and microcubes and their enhanced formaldehyde gas sensing performance
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Porous NiO/SnO2 microspheres and microcubes were obtained using a facile chemical solution route combined with a subsequent calcination process. The morphologies and crystal structures of the products were comprehensively characterized via X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, thermogravimetric-differential thermal analysis, and Brunauer-Emmett-Teller N2 adsorption-desorption analyses. The process of inducing porosity began with the NiSn(OH)6 precursors formed by the co-precipitation of the metal ions from the aqueous solution. Thermal decomposition of the precursors led to an intimate mixture of cubic phase NiO and tetragonal phase SnO2 and formed the porous NiO/SnO2 microspheres and microcubes. The gas-sensing properties of the as-prepared porous NiO/SnO2 microspheres and microcubes for toxic volatile organic compounds (VOCs), such as formaldehyde, ethanol, benzene, methanol, acetone, and toluene, were investigated. Compared with other VOCs gases, the porous NiO/SnO2 microsphere and microcube sensors exhibited a high response to formaldehyde. As for the porous NiO/SnO2 microsphere sensor, the detection limit of formaldehyde was approximately 0.13Â ppm (signal-to-noise ratio, S/NÂ =Â 3). The relationship between the gas-sensing performance and the microstructure of the porous NiO/SnO2 micro/nanomaterials was also discussed.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Sensors and Actuators B: Chemical - Volume 241, 31 March 2017, Pages 298-307
Journal: Sensors and Actuators B: Chemical - Volume 241, 31 March 2017, Pages 298-307
نویسندگان
Cuiping Gu, Yanwei Cui, Liyou Wang, Enhong Sheng, Jae-Jin Shim, Jiarui Huang,