| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 10540513 | Food Chemistry | 2013 | 7 Pages |
Abstract
⺠A method was developed to allow quantification of sulforaphene in samples by HPLC analysis. ⺠A suitable two-phase solvent system was optimised for preparative HSCCC. ⺠An acceptable sample loading amount was optimised for preparative HSCCC. ⺠249.4 mg of pure sulforaphene was obtained with preparative HSCCC by one-step separation. ⺠The purified product was characterised as sulforaphene by MS, 1H NMR, 13C NMR and DEPT-135 NMR.
Related Topics
Physical Sciences and Engineering
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Analytical Chemistry
Authors
Pengqun Kuang, Dan Song, Qipeng Yuan, Xinhua Lv, Di Zhao, Hao Liang,