Article ID Journal Published Year Pages File Type
10540987 Food Chemistry 2012 12 Pages PDF
Abstract
► A Validated LC-MS/MS method for ergot alkaloids in food and feed is proposed. ► The method allows simultaneous determination of major ergot alkaloids and epimers. ► Stability of XBridge column under alkaline conditions allows improved chromatography. ► The sample preparation protocol allows minimising analyte epimerization. ► Ergot alkaloids were present (1-1145 μg/kg) in Belgian food and feed commodities.
Keywords
Related Topics
Physical Sciences and Engineering Chemistry Analytical Chemistry
Preview
Development and validation of a new LC-MS/MS method for the simultaneous determination of six major ergot alkaloids and their corresponding epimers. Application to some food and feed commodities
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