Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
10548049 | Journal of Chromatography A | 2005 | 8 Pages |
Abstract
A method was developed for extracting, identifying, and quantifying diphenylamine (DPA) derivatives in the peel of DPA-treated apples using gradient reversed-phase liquid chromatography with ultraviolet-visible absorption and atmospheric pressure chemical ionization detection (LC-UV-vis-APCI-MS). Compounds routinely analyzed using this method included hydroxylated, nitrosated, nitrated, and methoxylated diphenylamine derivatives. Analysis of peel treated with 0-8 g Lâ1 DPA showed that peel DPA content was a limiting factor in derivative production and that recovery of most compounds over this range was linear.
Keywords
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
David R. Rudell, James P. Mattheis, John K. Fellman,