Article ID Journal Published Year Pages File Type
10638147 Materials Chemistry and Physics 2011 7 Pages PDF
Abstract
Composite polyvinyl amine/SBA-15 (PVAm/SBA-15) in various amounts of SBA-15 were prepared and characterized. The physical and chemical properties of PVAm/SBA-15 were investigated using FT-IR, XRD, BET, SEM and TGA techniques. The catalytic performance of each material was determined for the Knoevenagel condensation reaction between carbonyl compounds and ethyl cyanoacetate in the presence of ethanol as solvent. The effects of reaction temperature, solvent and the amounts of catalyst as well as recyclability of the catalyst were investigated. The catalyst used for this synthetically useful transformation showed a considerable degree of reusability besides being very active.
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Physical Sciences and Engineering Materials Science Electronic, Optical and Magnetic Materials
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