Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
11032082 | Results in Physics | 2018 | 17 Pages |
Abstract
The effect of quenching and annealing heat treatment on the localized corrosion resistance of 301 austenitic steel in 2â¯M H2SO4/0.75%-2.25% NaCl was studied by potentiodynamic polarization, open circuit potential measurement and optical microscopy analysis. The corrosion rate of the quenched, annealed and untreated steel increased with increase in NaCl concentration. The quenched steel had the lowest corrosion rate values, followed by the annealed steel. Variation in Clâ ion concentration had no significant effect on the pitting corrosion resistance and passivation behavior of the quenched steel, though increase in current density at breakdown potential was observed at higher Clâ ion concentration. The untreated steel experienced significant reduction and collapse of it passive film after 1.5% NaCl. Delayed passivation occurred on the annealed steel following metastable pitting lead to short passivation range. Open circuit potential measurement showed large cathodic shift of the corrosion potential for the quenched steel, compared to the anodic shift for the untreated steel. Optical microscopic images showed a deteriorated morphology and the presence of different phases for the untreated 301SS. Intergranular cracks were observed on the annealed and quenched 301SS while corrosion pits was observed on the annealed 301SS.
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Authors
Roland Tolulope Loto, Cleophas Akintoye Loto, Idehai Ohijeagbon,