Article ID Journal Published Year Pages File Type
1204293 Journal of Chromatography A 2013 12 Pages PDF
Abstract
► Clean and easy derivatization for identification of cyanide. ► By 19F{1H} NMR (without any sample cleanup), online LC-UV-SPE-offline 1H NMR experiments. ► Additionally GC-MS & GC-FTIR experiments were also performed to confirm the identity of the derivative. ► HPLC separation under gradient elution, using non-deuterated solvents. ► Yields clean and reproducible 19F{1H}, 1H NMR spectra and HPLC traces.
Related Topics
Physical Sciences and Engineering Chemistry Analytical Chemistry
Authors
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