Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1204293 | Journal of Chromatography A | 2013 | 12 Pages |
Abstract
⺠Clean and easy derivatization for identification of cyanide. ⺠By 19F{1H} NMR (without any sample cleanup), online LC-UV-SPE-offline 1H NMR experiments. ⺠Additionally GC-MS & GC-FTIR experiments were also performed to confirm the identity of the derivative. ⺠HPLC separation under gradient elution, using non-deuterated solvents. ⺠Yields clean and reproducible 19F{1H}, 1H NMR spectra and HPLC traces.
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
Avik Mazumder, Ajeet Kumar, Devendra K. Dubey,