Article ID Journal Published Year Pages File Type
1213711 Journal of Chromatography B 2010 5 Pages PDF
Abstract

The arctiin and arctigenin in the fruit of Arctium lappa L. were extracted by matrix solid-phase dispersion (MSPD) and determined by high-performance liquid chromatography (HPLC) with fluorescence detection. The experimental conditions for the MSPD were optimized. Silica gel was selected as dispersion adsorbent and methanol as elution solvent. The calibration curve showed good relationship (r > 0.9998) in the concentration range of 0.010–5.0 μg mL−1 for arctiin and 0.025–7.5 μg mL−1 for arctigenin. The recoveries were between 74.4% and 100%. The proposed method consumed less sample, time and solvent compared with conventional methods, including ultrasonic and Soxhlet extraction.

Related Topics
Physical Sciences and Engineering Chemistry Analytical Chemistry
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