Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1235118 | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy | 2007 | 6 Pages |
Abstract
The condensation reaction of {N-[(2-hydroxyphenylmethyl)amino]-4,6-dimethylpyridine} (2), which is a reduction product of 1, with trimer N3P3Cl6 affords partially a substituted spiro-cyclic phosphazene derivative (3). The fully substituted phosphazenes (4 and 5) have also been obtained from the reactions of 3 with the excess of pyrrolidine and morpholine. The characterizations and spectral investigations of these compounds have been made by elemental analyses, FTIR, 1H-, 13C-, 31P NMR, correlation spectroscopy (COSY), heteronuclear chemical shift correlation (HETCOR), heteronuclear multiple-bond correlation (HMBC) and mass spectroscopy (MS). The salient features of spectral data of these compounds have been discussed.
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Authors
Hakan Dal, Yasemin Süzen,