Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1253012 | Chemical Research in Chinese Universities | 2007 | 5 Pages |
Abstract
A novel flower-like hydrated magnesium carbonate hydroxide, Mg5 (CO3)4 (OH)2
- 4H2O, with micro-structure composed of individual thin nano-sheets was synthesized using a facile solution route without the use of template or organic surfactant. Reaction time has an important effect on the final morphology of the product. The micro-structure and morphology of Mg5 (CO3)4 (OH)2
- 4H2O were characterized by means of X-ray diffractometry (XRD), field-emission scanning electron microscopy (FE-SEM). Brunauer-Emmett-Teller (BET) surface areas of the samples were also measured. The probable formation mechanism of flower-like micro-structure was discussed. It was found that Mg5 (CO3)4 (OH)2
- 4H2O with flower-like micro-structure was a novel and efficient catalyst for the synthesis of diphenyl carbonate (DPC) by transesterification of dimethyl carbonate (DMC) with phenol.
- 4H2O, with micro-structure composed of individual thin nano-sheets was synthesized using a facile solution route without the use of template or organic surfactant. Reaction time has an important effect on the final morphology of the product. The micro-structure and morphology of Mg5 (CO3)4 (OH)2
- 4H2O were characterized by means of X-ray diffractometry (XRD), field-emission scanning electron microscopy (FE-SEM). Brunauer-Emmett-Teller (BET) surface areas of the samples were also measured. The probable formation mechanism of flower-like micro-structure was discussed. It was found that Mg5 (CO3)4 (OH)2
- 4H2O with flower-like micro-structure was a novel and efficient catalyst for the synthesis of diphenyl carbonate (DPC) by transesterification of dimethyl carbonate (DMC) with phenol.
Related Topics
Physical Sciences and Engineering
Chemistry
Chemistry (General)
Authors
WANG Qiang, WANG Ke-li, WU Xing-long, LUO Sheng-jun, HU Chang-wen,