Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1271482 | Ultrasonics Sonochemistry | 2006 | 9 Pages |
Abstract
The influence of several experimental parameters on the ultrasonic extraction of Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and solvent polarity. The optimized procedure employed 5 g of ground flowers, 150 mL of methanol and 140 min of extraction. The extracts were fractionated using preparative silica columns and the resulting fractions were analyzed by GC/MS. Some saturated hydrocarbons, fatty acids, fatty acid methyl esters, phytosterols, and vitamin E were identified in the plant extracts.
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Physical Sciences and Engineering
Chemistry
Chemistry (General)
Authors
Maria Inês Soares Melecchi, Valéria Flores Péres, Cláudio Dariva, Claudia Alcaraz Zini, Fernanda Contieri Abad, Migdália Miranda Martinez, Elina Bastos Caramão,