Article ID Journal Published Year Pages File Type
1298430 Solid State Ionics 2006 5 Pages PDF
Abstract

Different morphological MoO2 nano-sized particles were synthesized by a low temperature hydrothermal reaction as a novel method. The physical characterizations were carried out by IR, TG/DTA, XRD, XPS, SEM, TEM and SAED. XRD and XPS data indicate the as-prepared samples present at pure phase MoO2 with monocline symmetry. Spherical, sheet-like and bar-shaped nano-particles are observed by SEM, respectively. The lithium-intercalation properties of spherical MoO2 powders were investigated by XRD, TEM and SAED in the light of bulk MoO2. The results showed an irreversible phase transition after the initial discharge process, which is obviously different from the bulk sample.

Related Topics
Physical Sciences and Engineering Chemistry Electrochemistry
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