Article ID Journal Published Year Pages File Type
1308008 Inorganica Chimica Acta 2010 6 Pages PDF
Abstract

A new nano-sized lead(II) coordination polymer of maleic acid (H2Mal), [Pb(μ7-Mal)]n (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other. After calcination of nano-sized compound 1 at 600 °C, pure phase micro-sized lead(II) oxide has been produced.

Graphical abstractA new nano-sized lead(II) coordination polymer of maleic acid (H2Mal), [Pb(μ7-Mal)]n (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other.Figure optionsDownload full-size imageDownload as PowerPoint slide

Related Topics
Physical Sciences and Engineering Chemistry Inorganic Chemistry
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