| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 1311326 | Inorganica Chimica Acta | 2010 | 4 Pages |
Abstract
Treatment of LiC6F5 with B(C6F5)3 in equal volumes of light petroleum and diethyl ether at low temperature followed by slow warming to room temperature precipitates a microcrystalline solid which dries under vacuum to a material with the composition [Li(OEt2)3][B(C6F5)4]. Crystallization from diethyl ether yields solvent dependent [Li(OEt2)4][B(C6F5)4], which has been crystallographically characterised.
Graphical abstractTreatment of LiC6F5 with B(C6F5)3 in light petroleum and diethyl ether at low temperature followed by crystallization yields solvent dependent [Li(OEt2)4][B(C6F5)4] which is readily converted to a material with the composition [Li(OEt2)3][B(C6F5)4].Figure optionsDownload full-size imageDownload as PowerPoint slide
Related Topics
Physical Sciences and Engineering
Chemistry
Inorganic Chemistry
Authors
Eddy Martin, David L. Hughes, Simon J. Lancaster,