Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1325239 | Journal of Organometallic Chemistry | 2009 | 4 Pages |
Synthesis of metal–organic framework (MOF) based on tetra-pyridyl porphyrin and palladium (II) salt resulted in the formation of palladium oxide nano-crystals. The palladium oxide nano-crystals were characterized by PXRD, TEM, HRTEM, ED, UV–Vis spectroscopy, DLS, SEM and AFM. A plausible mechanism for the in situ generation of nano-crystals has been proposed.
Graphical abstractPalladium oxide nano-crystal formed in the synthesis of metal–organic framework (MOF) based on tetra-pyridyl porphyrin and palladium. The palladium oxide nano-crystals were characterized by PXRD, TEM, HRTEM, ED, UV–Vis, DLS, SEM and AFM. A plausible mechanism for the in situ generation of nano-crystals has been proposed.Figure optionsDownload full-size imageDownload as PowerPoint slide