| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 1332764 | Journal of Solid State Chemistry | 2006 | 5 Pages |
A novel intercalated borate compound (NH3CH2CH2NH3)B6O9(OH)2, has been solvothermally synthesized, and structurally characterized by single crystal X-ray diffraction. Compound crystallizes in the monoclinic, space group P 2(1)/c, a=8.6200(17)Å, b=15.656(3)Å, c=8.8386(18)Å, β=93.32(3)°β=93.32(3)°, V=1190.8(4)Å3, Z=4Z=4. Its oxoborate structure is built up from 1-D polyborate chains with 3, 11-membered boron rings bonded diamine molecules through electrostatic attraction and hydrogen bond interactions to construct 2-D layered compound. Other characterizations by IR, element analysis, thermal analysis and specific surface area are also discussed.
Graphical abstractA novel intercalated borate compound (NH3CH2CH2NH3)B6O9(OH)2, has been solvothermally synthesized, and structurally characterized.Figure optionsDownload full-size imageDownload as PowerPoint slide
