Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1389184 | Carbohydrate Research | 2007 | 5 Pages |
Abstract
Microwave heating was applied to the reactions involved in the synthesis of 6-amino-6-deoxycellulose, 4. These included, cellulose solubilization, bromination at C-6, displacement of bromine with azide ion, and reduction of the azido group to an amino group. Compared to conventional heating, this approach had the advantages of shortening reaction times and retaining the degree of polymerization of 4.
Graphical abstractMicrowave heating had the advantages of shortening reaction times and retaining of the degree of polymerization of cellulose derivatives in the synthesis of 6-amino-6-deoxycellulose.Figure optionsDownload full-size imageDownload as PowerPoint slide
Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Toshiyuki Takano, Junya Ishikawa, Hiroshi Kamitakahara, Fumiaki Nakatsubo,