Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1390831 | Carbohydrate Research | 2007 | 8 Pages |
Abstract
The synthesis of (4,5,6-13C)-deoxymannojirimycin is described. The route employed is based on Sharpless asymmetric epoxidation of (1,2,3-13C)(E)-2,4-pentadien-1-ol and uses ring-closing metathesis as a key step. The labeled compound may be easily used for protein-binding experiments using NMR spectroscopic methods.
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Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Caterina Murruzzu, Mònica Alonso, Angeles Canales, Jesus Jiménez-Barbero, Antoni Riera,