Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1476573 | Journal of the European Ceramic Society | 2011 | 11 Pages |
Abstract
A preferential orientation was observed in a Sm-sialon ceramic, of the composition Sm0.4Si9.6Al2.4O1.2N14.8, after hot pressing at 1800 °C for 2 h. Post-sintering heat treatment was performed at 1450 °C for 384 h, resulting in the forward αâ²Â â βⲠtransformation, accompanied by the formation of Mâ²SS and an increase in the 21R phase. Subsequent heat treatment at 1800 °C for 2 h resulted in the reverse βâ²Â â αⲠtransformation, with a corresponding decrease in the Mâ²SS and 21R phases. This confirms the fully reversible reaction of αâ²+liquidâβâ²+Mâ²SS+21R in Sm-sialon ceramics. In addition, the texture introduced by hot pressing was maintained after all heat treatments, indicating that there is a crystallographic relationship between the transformation phases. The microstructure and mechanical properties were also found to be mostly reversible, contrary to the behaviour of the αⲠlattice parameters and bulk density.
Related Topics
Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Andrew Carman, Elena Pereloma, Yi-Bing Cheng,