Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1489132 | Materials Research Bulletin | 2012 | 5 Pages |
In the present study, we report, for the first time, the synthesis of cobalt oxyhydroxide thin films on inexpensive stainless steel substrate using potentiodynamic electrodeposition method. These films were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM) techniques. The orthorhombic crystal structure was revealed by the X-ray diffraction study. The FT-IR spectrum confirmed the formation of cobalt oxyhydroxide. The SEM studies showed the nanoflakes-like morphology with an average thickness of 100 nm. The cyclic voltammetry study of the cobalt oxyhydroxide films in 1 M KOH showed maximum specific capacitance of 449 F g−1 at scan rate of 5 mV s−1.
Graphical abstractScanning electron micrograph (SEM) images of cobalt oxyhydroxide thin film at (a) 2000× and (b) 10,000× magnifications.Figure optionsDownload full-size imageDownload as PowerPoint slideHighlights► Simple method for the synthesis of CoOOH thin films. ► Supercapacitor with maximum specific capacitance of 449 F g−1. ► High charge/discharge efficiency.