Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1489893 | Materials Research Bulletin | 2013 | 4 Pages |
The face-centered tetragonal (FCT) ordered L10 CoPt nanoparticles (NPs) are prepared by the sol–gel method. Their structure and magnetic properties are characterized by the X-ray diffraction (XRD), the transmission electron microscope (TEM) and the vibrating sample magnetometer (VSM). The results indicate that the CoPt NPs heated at 400 °C are the disordered face-centered cubic (FCC) structure, whereas the samples annealed at the temperature above 600 °C exhibit an ordered FCT structure. TEM images show the increase of the particle size as the annealing temperature increases. SAED images show the appearance of the L10 phase at 800 °C, and the maximum coercivity is 254,720.3 A/m.
Graphical abstractCoPt NPs are successfully synthesized by sol–gel method. Different distinct particle sizes with narrow particle size distribution of CoPt nanoparticles are obtained. The maximum coercivity of 254,720.3 A/m is obtained for 800 °C heat-treated sample.Figure optionsDownload full-size imageDownload as PowerPoint slideHighlights► L10-CoPt NPs with FCT structure are successfully synthesized by sol–gel method. ► The maximum value of 254,720.3 A/m is obtained for the samples heated at 800 °C. ► The synthetic route proposed in this study is less toxic and easy-to-handle.