Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1491827 | Materials Research Bulletin | 2008 | 6 Pages |
Abstract
Nanocrystalline Prussian Blue analogue Ni2[Fe(CN)6]·xH2O was synthesized through hydrothermal process at 180 °C for 24 h with NiSO4·6H2O and K4[Fe(CN)6]·3H2O as precursors. The effects of reactant concentration and protective matrix (Polyethylene glycol 400, PEG-400) on the size and morphology of nanoparticles were investigated. The as-synthesized products were identified as face-centered cubic structure by powder X-ray diffraction. Field-emission scanning electron microscopy and transmission electron microscopy images showed that well dispersed nanoparticles with fairly narrow size distribution were successfully prepared.
Keywords
Related Topics
Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Shaohua Xu, Xuefeng Qian, Gang Li,