| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 1492727 | Materials Research Bulletin | 2006 | 7 Pages |
Abstract
The ferroelectric layered Bi5Ti3FeO15 and LaBi4Ti3FeO15 Aurivillius phases were synthesized in high purity and textured microstructures in a molten Na2SO4/K2SO4 (1:1 molar ratio) flux in much shortened reaction times, 1 h minimum compared to conventional techniques. The particle growth and microstructure of both phases were investigated as a function of temperature and reaction duration, and yielded plate-like particles that could be synthesized in sizes from <1 μm to >20 μm. The product crystallinity, purity and microstructures were characterized via powder X-ray diffraction and scanning electron microscopy. The UV–vis diffuse reflectance of the products were measured and analyzed with respect to the resultant particle sizes.
Related Topics
Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Digamber G. Porob, Paul A. Maggard,