Article ID Journal Published Year Pages File Type
1500767 Scripta Materialia 2010 4 Pages PDF
Abstract

A novel set-up developed to continuously observe and measure stress-driven grain boundary migration is presented. A commercial tensile/compression scanning electron microscope hot stage was utilized for in situ observations of mechanically loaded samples at elevated temperatures up to 850 °C by recording orientation contrast images of bicrystal surfaces. Two sample holders were designed and fabricated for applying a shear stress to the boundary in bicrystals of various geometries. The results of the first measurements in Al bicrystals are presented.

Related Topics
Physical Sciences and Engineering Materials Science Ceramics and Composites
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