Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1507120 | Solid State Sciences | 2006 | 5 Pages |
Abstract
The fast thermolysis of ammonium molybdate leads to a mixture of MoO3 and Mo5.3O14.5(OH)2.8(H2O)1.36 with spherical and rod-like morphologies. The oxide mixture can be converted in quantitative yield to inorganic fullerene-type (IF) MoS2 and MoS2 nanotubes (NT) by H2S reduction using a facile and quick procedure. The products were studied by X-Ray Diffraction (XRD) and by Transmission Electron Microscopy (TEM). TEM analysis reveals that the spherical and rod-like morphology of the oxide precursor is preserved during the H2S treatment.
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Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Helen A. Therese, Nicole Zink, Ute Kolb, Wolfgang Tremel,