Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1516972 | Journal of Physics and Chemistry of Solids | 2011 | 5 Pages |
Microwave-assisted synthesis is a novel method used to synthesize CdMoO4 nanoparticles in propylene glycol. The effects of reaction time and microwave power on phase, morphologies, and optical properties of CdMoO4 nanoparticles were studied, using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and UV–visible spectroscopy. The present analyses proved that these crystalline powders were scheelite-type tetragonal structured CdMoO4, with the crystallite size of 14–20 nm, and 4.51–4.73 eV band gaps, controlled by the synthetic conditions.
Research highlights► Microwave-assisted synthesis is a novel method used to synthesize CdMoO4 nanoparticles in propylene glycol. ► The effects of reaction time and microwave power on phase, morphologies, and optical properties of CdMoO4 nanoparticles were studied and discussed in this paper.