Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1519041 | Journal of Physics and Chemistry of Solids | 2006 | 4 Pages |
Abstract
Electrochemical formation of graphite intercalation compounds in H2SO4-[1-14C] CH3COOH solutions was studied by radiotracer analysis coupled with autoradiography. It was shown that a stage 1 ternary graphite intercalation compound (TGIC) can be synthesized in 60 and 80% H2SO4. The only formation of graphite bisulfate (GB) was observed in 20 and 40% H2SO4. The presence of ethanoic acid in the graphite matrix was confirmed by thermogravimetry coupled with mass-spectrometry and Fourier IR-spectroscopy.
Keywords
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Physical Sciences and Engineering
Materials Science
Electronic, Optical and Magnetic Materials
Authors
N.V. Maksimova, V.S. Leshin, V.V. Avdeev, N.E. Sorokina,