Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1530266 | Materials Science and Engineering: B | 2009 | 5 Pages |
Abstract
Hydroxyapatite prepared by sol–gel route was investigated with respect to local structure changes induced by heat treatment. The X-ray diffraction analysis revealed the presence of nanocrystalline hydroxyapatite with significantly broadened reflections for the sample dried at 110 °C as compared with the samples heat treated at 900 °C and 1150 °C. Line broadenings for the nanocrystalline sample are evidenced also in the X-ray photoelectron spectroscopy and nuclear magnetic resonance spectra. By heat treatment at high temperatures the atomic environment is modified both around cations and oxygen. A higher bioactivity is expected from the nanocrystalline sample than from the high temperature heated samples with large sized crystals.
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Authors
V. Simon, D. Lazăr, R.V.F. Turcu, H. Mocuta, K. Magyari, M. Prinz, M. Neumann, S. Simon,