Article ID Journal Published Year Pages File Type
1570879 Materials Characterization 2015 6 Pages PDF
Abstract

•An Fe–6.5 wt.% Si as-cast strip doped with cerium was produced.•A thin warm rolled sheet with limited edge cracks was obtained.•Microstructure and texture evolution at each stage were investigated.•Strong λ-fiber and Goss recrystallization textures were formed.•The magnetic properties of the annealed sheet were significantly improved.

A 0.3 mm thick non-oriented 6.5 wt.% Si electrical steel sheet doped with cerium is produced by twin-roll strip casting, hot rolling, warm rolling and annealing. A detailed study of the cerium precipitates in the as-cast strip, microstructure and texture evolution at different processing stages is carried out by electron probe micro-analysis, optical microscopy, X-ray diffraction and electron backscattered diffraction analysis. Grain interior distributing precipitates identified as Ce-oxides, Ce-oxysulfides and Ce-phosphides, and boundary distributing Ce-oxides and Ce-phosphides are observed in the as-cast strip. The initial as-cast strip is characterized by a much finer solidification microstructure and dominated by obvious < 001 >//ND texture through the strip thickness. After hot and warm rolling, inhomogeneous microstructure containing large amounts of in-grain shear bands is characterized by mixed < 110 >//RD and < 111 >//ND textures. The texture of the annealed sheet with a relatively large average grain size is far more optimized by the domination of the beneficial cube, rotated cube, {001}< 120 > to {001}< 130 > and Goss texture components, and the elimination of the detrimental γ-fiber texture, leading to a superior magnetic induction and improved iron loss.

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Physical Sciences and Engineering Materials Science Materials Science (General)
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