Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1571839 | Materials Characterization | 2009 | 5 Pages |
Abstract
Nanocrystalline Nd2(Zr1 − xSnx)2O7 series solid solutions were prepared by a convenient salt-assisted combustion process using glycine as fuel. The samples were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, Raman spectroscopy, transmission electron microscopy and high-resolution transmission electron microscopy. The results showed the Zr ion can be partially replaced by Sn ion. The partial substituted products were still single-phase solid solutions and the crystal form remained unchanged. TEM images reveal that the products are composed of well-dispersed square-shaped nanocrystals. The method provides a convenient and low-cost route for the synthesis of nanostructures of oxide materials.
Keywords
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Physical Sciences and Engineering
Materials Science
Materials Science (General)
Authors
Yuping Tong, Yanping Wang,