Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1652854 | Materials Letters | 2007 | 4 Pages |
Abstract
C3N4 nanowires and pseudocubic C3N4 polycrystalline nanoparticles have been synthesized by the reaction between C3N3Cl3 and NaN3 with Zn powder as catalyst. The process was carried out using a constant-pressure benzene thermal method at 40 MPa and 220 °C. The prepared nanowires have a diameter range of 3–6 nm and length range of 100–200 nm, while the diameters of the nanoparticles range from 10 nm to 40 nm. The as-prepared samples were characterized by X-ray powder diffraction (XRD), Fourier transform spectroscopy (FTIR), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and X-ray photoelectron spectroscopy (XPS).
Related Topics
Physical Sciences and Engineering
Materials Science
Nanotechnology
Authors
Xifeng Lu, Ligang Gai, Deliang Cui, Qilong Wang, Xian Zhao, Xutang Tao,