Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1665999 | Thin Solid Films | 2013 | 5 Pages |
Abstract
Continuous indium metal-organic framework thin films of In12O(OH)12[(OH)4·(H2O)5)][BTC]6 (MIL-96(In)) (BTC = 1,3,5-benzenetricarboxylate) were prepared on indium tin oxide glass by in situ solvothermal growth method. The structure of the films was confirmed by X-ray diffraction. The growth process and the possible growth mechanism of MIL-96(In) films were investigated by a scanning electron microscopy. Furthermore, the influence of the reaction conditions on the morphology and thickness of films was studied. The best crack-free, continuous film with thickness of approximate 6 μm was obtained at the proper concentrations of InCl3 and H3BTC of 25.0 mmol·lâ 1 at 100 °C for 12 h.
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Authors
Zhongshang Dou, Jiancan Yu, Hui Xu, Yuanjing Cui, Yu Yang, Guodong Qian,