Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1688557 | Vacuum | 2014 | 6 Pages |
Abstract
Separation and recovery process of zinc from scrap copper-based alloy was carried out under vacuum condition in a sublimation reactor. The factors affecting the evaporation ratio of copper-based alloy and the separation efficiency of zinc, such as heating temperature, residual gas pressure, vacuum evaporation time and the amount of scrap copper-based alloy were separately investigated. The experimental results revealed that zinc was successfully separated from the scrap copper-based alloy, where the evaporation ratio of copper-based alloy reached 18.43%. Namely, 96.09% by weight of zinc could be removed under the condition: residual gas pressure of 50Â Pa, heating temperature of 1323Â K and vacuum evaporation time of 90Â min. If corresponding to the residual gas pressure 500Â Pa, the evaporation ratio reached 18.17%, and 94.73% by weight of zinc could be removed under the following experimental conditions: temperature 1323Â K, vacuum evaporation time 180Â min. Meanwhile, the thermodynamics of vacuum sublimation and refining to recover zinc was analyzed and calculated.
Keywords
Related Topics
Physical Sciences and Engineering
Materials Science
Surfaces, Coatings and Films
Authors
Yunjian Ma, Keqiang Qiu,