| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 1694487 | Applied Clay Science | 2015 | 8 Pages |
Abstract
In this work, the influence of the zinc content and synthesis methodology on the physicochemical properties of mixed oxide derivatives from the hydrotalcite precursor MgZnAl-HT were evaluated. Layered double hydroxides (LDH) were prepared by co-precipitation, ultrasound and urea hydrolysis methods followed by calcination at 500 °C. The materials were studied by such techniques as inductively coupled plasma, X-ray powder diffraction, Raman spectroscopy and 27Al solid-state NMR spectroscopy. The textural and morphological properties of mixed oxides were evaluated through the adsorption/desorption of N2 and scanning electron microscopy (SEM). Different textural and morphological properties were observed for the samples.
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Authors
Weberton Reis do Carmo, Juliana Fischer-Haddad, Luciano Honorato Chagas, Marilia S.S. Beltrão, Gustavo S.G. de Carvalho, Luiz Carlos A. de Oliveira, Talita E. Souza, Alexandre Amaral Leitão, Renata Diniz,