Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1799033 | Journal of Magnetism and Magnetic Materials | 2015 | 5 Pages |
•CoFe2O4 nanospheres were prepared by hydrothermal synthesis for the first time.•Average grain size was found to be 180 nm.•Its structural, morphological, magnetic behavior was studied.•TEM observations confirmed the spherical morphology of the mesoporous ferrites.
Mesoporous CoFe2O4 nanospheres with an average size of 180 nm were fabricated via a facile hydrothermal process using ethylene glycol as solvent and sodium acetate (NaAc) as electrostatic stabilizer. In this method, ethylene glycol plays a vital role in the formation of cobalt nanoospheres as a solvent and reducing agent. The structure and morphology of the prepared materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution TEM (HRTEM), Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS). The nanospheres exhibited ferromagnetic properties with high saturation magnetization value of about 60.19 emu/g at room temperature. The BET surface area of the nanospheres was determined using the nitrogen absorption method. The porous CoFe2O4 nanospheres displayed good magnetic properties, which may provide a very promising candidate for their applications in target drug delivery.