Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
186373 | Electrochimica Acta | 2014 | 9 Pages |
Abstract
The results of an experimental study on electrochemical preparation of polyaniline (PANI)/polycrystalline gold composites are reported in this work. A three steps approach is adopted in order to obtain a stable and uniform coating: (1) functionalization of the gold surface by 4-nitrophenyl group, (2) electrochemical reduction of the nitro group to amine, and (3) electropolymerization of aniline onto the surface of the aminophenyl-modified gold electrode. Cyclic voltammetries and electrochemical impedance spectroscopies are used to characterize the gold surface after each step. Also the results of a sample prepared by electropolymerization of PANI on bare gold are presented as a comparison.
Related Topics
Physical Sciences and Engineering
Chemical Engineering
Chemical Engineering (General)
Authors
A. Vacca, M. Mascia, S. Rizzardini, S. Palmas, L. Mais,