Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
2058706 | MethodsX | 2014 | 7 Pages |
Abstract
A combined procedure for separating Fe and Hf from a single rock digestion is presented. In a two-stage chromatographic extraction process, a purified Fe fraction is first quantitatively separated from the rock matrix using AG-MP-1M resin in HCl. Hafnium is subsequently isolated using a modified version of a commonly applied method using Eichrom LN-Spec resin. Our combined method includes:•Purification of Fe from the rock matrix using HCl, ready for mass spectrometric analysis.•Direct loading of the matrix onto the resin that is used for Hf purification.•Collection of a Fe-free Hf fraction.
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Authors
Ting Cheng, Oliver Nebel, Paolo A. Sossi, Fukun Chen,