High-pressure compaction modelling of calcite (CaCO3) powder compact

Numerical simulation of manufacturing processes with working conditions at high pressure (above 1 GPa) requires constitutive data of the powder for the whole range of pressure and density. Most of the test apparatuses commonly used to obtain such data are only working in the lower pressure regions. Because of the absence of high-pressure data, many parameters have to be guessed or extrapolated. A material used in high-pressure applications is Calcite (CaCO3). The material can be used as an insulator in high-pressure capsules it is also a common material in the earth core. An apparatus often used to generate high pressure during compaction is the Bridgman anvil apparatus. In this work experimental tests with a Bridgman anvil set-up using Calcite powder discs with different thicknesses were done. A nonlinear elastic-plastic cap model was developed to model the behaviour of powder material from low pressure and loose state to high pressure and solid state. The constitutive model was implemented in a finite element code. The constitutive data were identified by optimization of experimental data. Validation was done by numerically reproduce the mechanical behaviour of uni-axially pressing Calcite to different pressure (up to 5 GPa) including unloading. The load–displacement curves, density distribution and the surface displacement were measured and compared to the finite element results. The results of the compaction simulations agree reasonably well with the experimental results.

Graphical AbstractThe aim of this paper is to develop a constitutive model for high-pressure compaction of Calcite (CaCO3) powder. A constitutive model was calibrated using material data determined from experiments. The compaction of CaCO3 powder discs, with two different thicknesses, was simulated using the FE method. Corresponding experiments were carried out using the Bridgman anvil apparatus. Results from simulations were compared to measured experimental results. The load-displacement curves, density distribution and the surface displacement were measured and compared with finite element simulations.Figure optionsDownload full-size imageDownload as PowerPoint slide