Article ID Journal Published Year Pages File Type
4701187 Chemical Geology 2007 14 Pages PDF
Abstract

40Ar–39Ar dating requires precise and accurate age data of standard fluence monitors. Besides primary calibration of K and 40Ar concentrations (i.e. the ages are calculated with precise K–Ar dating), intercalibration of the different monitors in use provides important cross-checks of the validity of standard ages and, implicitly, reliability and uncertainty of chronological studies that rely on these standards. Here we report intercalibration of 5 primary international 40Ar–39Ar standards and one internal laboratory monitor. A major goal of this study was to check the ages of the NL-25 hornblende standard and of the muscovite laboratory standard BMus/2 against the international standards HD-B1, GA1550, SB-3 and HB3gr. In replicate measurements of three irradiation series, 40Ar–39Ar ages for the fluence monitors were found which agree within 1σ-error limits with the reported age values of 2660 ± 9 Ma for NL-25, Hb3gr: 1073.6 ± 4.6 Ma, BMus/2: 328.5 ± 1.1 Ma, SB-3: 162.9 ± 0.8, GA1550: 98.79 ± 0.54 and 24.21 ± 0.32 for HD-B1. For the hornblende NL-25 fluence monitor a new – slightly different – 40Ar–39Ar age of 2657 ± 4 Ma is suggested. For the age of the muscovite BMus/2 laboratory standard we recommend 328.5 ± 1.1 Ma, and for biotite HD-B1 a more precise value of 24.18 ± 0.09 Ma.

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