Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5135884 | Journal of Chromatography A | 2016 | 11 Pages |
Abstract
The results reveal that (1) the column efficiency can be maximized by properly selecting the difference between the eluent and the oven temperatures, (2) the mere wrapping of the column with an excellent insulating material is insufficient to fully eliminate heat exchanges by conduction and the undesirable radial density gradients across the column i.d., and (3) the complete thermal insulation of the SFC column under high vacuum allows to maximize the column efficiency by maintaining the integrity of the peak shape.
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
Fabrice Gritti, Michael Fogwill, Martin Gilar, Joseph A. Jarrell,