Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5139269 | Microchemical Journal | 2017 | 8 Pages |
Abstract
The resultant core-shell magnetic solid-phase extraction nanoparticle sorbent was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), vibrating sample magnetometer (VSM) and Fourier transform-infrared (FT-IR) spectroscopy. The dominant parameters affecting enrichment efficiency were investigated and optimized. Under the optimum conditions detection limits and linear dynamic ranges were achieved in the range of 0.005-0.02 ng mLâ 1 and 0.02-200 ng mLâ 1, respectively. The relative standard deviations (RSDs) for five replicates at three concentration levels (0.05, 5 and 100 ng mLâ 1) of analytes were ranged from 3.8 to 7.0%. Ultimately, the applicability of this method was successfully confirmed by analyzing tap, well, sea and waste water samples and satisfactory results were obtained.
Keywords
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
Ebrahim Ebrahimpour, Amirhassan Amiri, Mehdi Baghayeri, Mona Rouhi, Moslem Mansour Lakouraj,