Improved synthesis of glycine, taurine and sulfate conjugated bile acids as reference compounds and internal standards for ESI-MS/MS urinary profiling of inborn errors of bile acid synthesis

Article ID	Journal	Published Year	Pages	File Type
5142687	Chemistry and Physics of Lipids	2017	46 Pages	PDF

Keywords

MECN TUDCA CDCA KOH DCA EtOAc GlcA Na2SO4 DPPA TCDCA UDCA Hydrochloride acid GDCA TDCA GCDCA GUDCA TLCA ESI–MS/MS Et2O HSD3B7 EEDQ NaOH HCl TCA TLC TFA GCA DEPC HRMS N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline Ethyl acetate LCA Acetonitrile Chenodeoxycholic acid Deoxycholic acid Trifluoroacetic acid Taurodeoxycholic acid Tauroursodeoxycholic acid taurochenodeoxycholic acid Taurolithocholic acid Taurocholic acid Lithocholic acid Cholic acid Glycodeoxycholic acid Glycoursodeoxycholic acid Glycochenodeoxycholic acid glycolithocholic acid glycocholic acid Ursodeoxycholic acid Liver disease Diethyl ether Sodium sulfate High resolution mass spectrometry Methanol equivalent MeOH sodium hydroxide Potassium Hydroxide thin-layer chromatography

Related Topics

Physical Sciences and Engineering Chemistry Chemistry (General)

Improved synthesis of glycine, taurine and sulfate conjugated bile acids as reference compounds and internal standards for ESI-MS/MS urinary profiling of inborn errors of bile acid synthesis

Authors

Elena Donazzolo, Antonina Gucciardi, Daniela Mazzier, Cristina Peggion, Paola Pirillo, Mauro Naturale, Alessandro Moretto, Giuseppe Giordano,