Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5161789 | Organic Geochemistry | 2012 | 10 Pages |
Abstract
⺠Two new HPLC methods for purifying dinosterol from other sedimentary alcohols and sterols. ⺠δD range was 560Ⱐacross a sterol peak during RP-HPLC. ⺠Average yield 80% for RP-HPLC vs. 60% for two step HPLC method. ⺠Resolution of dinosterol optimized with a mid-polarity VF-17ms GC column. ⺠Dinosterol purified via the HPLC methods had reproducible and unbiased δD value.
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Authors
Alyssa R. Atwood, Julian P. Sachs,