Article ID Journal Published Year Pages File Type
5203996 Polymer Degradation and Stability 2009 18 Pages PDF
Abstract

Two silicone ceramer coatings were synthesized and studied according to their thermal stability, using Fourier Transformation Infra-red (FTIR) spectroscopy. Differential thermal analysis was conducted on a liquid precursor to the coatings to study the phase transformations occurring in the material as the temperature was altered. The kinetics of the thermal degradation of coatings was analyzed; and the corresponding thermokinetics parameters were determined using Friedman's method, the Flynn-Wall-Ozawa method and the American standard test method E698. A thermogravimetric analysis was conducted on the liquid precursors as well as on the solidified coatings at various heating rates. The gaseous products that were obtained as a result of pyrolysis were analyzed employing an attached FTIR spectrometer.

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Physical Sciences and Engineering Chemistry Organic Chemistry
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