Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5204808 | Polymer Degradation and Stability | 2006 | 4 Pages |
Abstract
A synthetic procedure based on thermal hydrolysis of iron(III) chloride solutions for the preparation of hematite (α-Fe2O3) sol consisting of nano-crystals (NCs) is described. The α-Fe2O3 NCs were characterized by transmission electron microscopy and X-ray diffraction measurements. Incorporation of α-Fe2O3 NCs into polystyrene (PS) was based on the transfer of α-Fe2O3 NCs from the aqueous phase to the organic solvent. A significant shift in the glass transition temperature of PS by 17 °C towards higher temperatures was observed after incorporation of α-Fe2O3 NCs. Also, the thermal stability of PS was improved by about 100 °C in the presence of 3.6 wt% of α-Fe2O3 NCs.
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Authors
Milena MarinoviÄ-CincoviÄ, Zoran V. Å aponjiÄ, Vladimir DjokoviÄ, Slobodan K. MilonjiÄ, Jovan M. NedeljkoviÄ,