Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5211930 | Tetrahedron | 2017 | 10 Pages |
Abstract
An efficient one-pot cascade methodology for the synthesis of (ethoxycarbonyl)difluoromethyl thioethers is described. Benzyl, allyl, alkyl halides or diazonium salts as the starting materials together with thiocyanate sodium and TMS-CF2CO2Et in the presence of CsF or NaOAc afford a variety of the fluoroalkylthiolated products in moderate to good yields.
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Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Lijun Xu, Hongyu Wang, Changwu Zheng, Gang Zhao,