Article ID Journal Published Year Pages File Type
5221151 Tetrahedron 2010 4 Pages PDF
Abstract

Microwave irradiation of a stoichiometric amount of Lawesson’s reagent in the presence of o-aminophenols, o-aminothiophenols, o-phenylenediamines, or catechols leads to benzoxazaphosphole-, benzothiazaphosphole-, benzodiazaphosphole-, and benzodioxaphosphole-2-sulfides, respectively, in good yields in a fast and direct way under solventless conditions. The procedure requires short reaction times and is similar for all reagents; thus it may be used in parallel synthesis.

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Related Topics
Physical Sciences and Engineering Chemistry Organic Chemistry