| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5228177 | Tetrahedron | 2008 | 6 Pages |
Abstract
Norcaran-2,3,4,5-tetraoles were synthesized starting from methyl 1,3,5-cycloheptatriene-7-carboxylate in several steps. Norcaradiene endoperoxide is the key component; it was obtained by photooxygenation of methyl 1,3,5-cycloheptatriene-7-carboxylate. The other oxygen functionalities are introduced through epoxide ring opening and OsO4-hydroxylation reactions.
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