| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5264547 | Tetrahedron Letters | 2013 | 5 Pages |
Abstract
A facile and efficient protocol for the oxidative deprotection of benzyl-type ethers has been developed. The reaction was performed with catalytic amounts of 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) and tert-butyl nitrite (TBN) under atmospheric pressure of O2. Under the optimal reaction conditions, a variety of PMB, PPB, and Bn ethers can be deprotected to their corresponding alcohols in excellent conversions and selectivities.
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Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Zhenlu Shen, Lili Sheng, Xiaochu Zhang, Weimin Mo, Baoxiang Hu, Nan Sun, Xinquan Hu,