| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5272111 | Tetrahedron Letters | 2009 | 4 Pages |
Abstract
The Stille cross-coupling reaction of [1-11C]acetyl chloride with tributylphenylstannane leading to [carbonyl-11C]acetophenone was studied. The coupled product [carbonyl-11C]acetophenone was synthesized in high radiochemical conversion from [1-11C]acetyl chloride using the Pd2(dba)3/P(MeNCH2CH2)3N·HCl system.
Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
![Synthesis of [carbonyl-11C]acetophenone via the Stille cross-coupling reaction of [1-11C]acetyl chloride with tributylphenylstannane mediated by Pd2(dba)3/P(MeNCH2CH2)3N·HCl](/preview/png/5272111.png "First Page Preview: Synthesis of [carbonyl-11C]acetophenone via the Stille cross-coupling reaction of [1-11C]acetyl chloride with tributylphenylstannane mediated by Pd2(dba)3/P(MeNCH2CH2)3N·HCl")
Authors
Takuya Arai, Koichi Kato, Ming-Rong Zhang,